3-甲基-3-丁烯-1-醇合成路线 (共 220 条)
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Justus Liebigs Annalen der Chemie, , vol. 630, p. 58 - 70
Journal of Biological Chemistry, , vol. 234, p. 2605
反应条件
magnesium in diethyl ether
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 32, # 1 p. 75 - 84
反应条件
T=200°C; P=320 - 640 Torr;
参考文献
Journal of the American Chemical Society, , vol. 77, p. 4666
反应条件
sodium hydroxide; dihydrogen peroxide; boron tribromide 1.) CH2Cl2, 0,5 h, -78 to 25 deg C, 2.) THF, 0,5 h, reflux; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 55, # 5 p. 1409 - 1410
反应条件
lithium aluminium tetrahydride Yield given;
参考文献
Tetrahedron Letters, , vol. 27, # 46 p. 5555 - 5558
反应条件
(2,6-di-tert-butyl-4-methylphenoxy)methylaluminum trifluoromethanesulfonate in dichloromethane T=25°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 23, # 18 p. 1933 - 1936
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); hydroxide; dihydrogen peroxide 1.) THF, r.t., 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 38, # 41 p. 7279 - 7282
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 227, p. 352
反应条件
4,4'-di-tert-butylbiphenylide; triethylaluminum 1) THF, -70 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 20 p. 5760 - 5761
反应条件
T=190°C; P=37 Torr; weitere Produkte: 4-Acetoxy-2-acetoxymethyl-but-1-en und 1,3-Diacetoxy-3-methyl-butan;
参考文献
Journal of the American Chemical Society, , vol. 77, p. 78