in pentane byproducts: (CH3)2NBF2; (N2); without moisture; added BF3 (cooling) to soln. of B-compound in pentane within 60 min; warmed; evapd. at -30°C; condensed at 25°C/10 Torr in -78°C cold vessel;
参考文献
Hoebel, Ulrike; Noeth, Heinrich; Prigge, Helene
Chemische Berichte, 1986 , vol. 119, # 1 p. 325 - 337
Witschonke, C. R.; Kraus, C. A.
Journal of the American Chemical Society, 1947 , vol. 69, p. 2472 - 2481
Full Text View citing articles Show Details
Gmelin Handbook: B: SVol.1, 4.4.5, page 187 - 196
absorbing of gaseous BF3 in cold methanol (molar ratio 1:1); fractional freezing;
参考文献
Greenwood, N. N.; Martin, R. L.
Journal of the Chemical Society, 1953 , p. 757 - 764
Full Text View citing articles Show Details
Gmelin Handbook: B: B-Verb.8, 5, page 73 - 90
