Colonge; Dumont
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1945 , vol. 220, p. 500
Bulletin de la Societe Chimique de France, 1947 , p. 38,44
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Eschenmoser et al.
Helvetica Chimica Acta, 1951 , vol. 34, p. 2329,2335
AlCl3 in neat (no solvent)
byproducts: CH3SiCl3; heated for 1 h to 125°C; stirred for 2 h; heated to 135-140°C and then at 145-150°C for 2 h; AlCl3 sepd.; vacuum-distd.; elem. anal.;
参考文献
Motsarev, G. V.; Chernyshev, E. A.; Rozenberg, V. R.; Inshakova, V. T.; Zetkin, V. I.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 985 - 988
Zhurnal Obshchei Khimii, 1988 , vol. 53, p. 1111 - 1114
in tetrahydrofuran
addn. of a soln. of SnCl4 to a soln. of organic compound under cooling, heating for 12 h under reflux; addn. of HCl, reccrystn., elem. anal.;
参考文献
Schneider-Koglin, Claudia; Mathiasch, Bernd; Draeger, Martin
Journal of Organometallic Chemistry, 1994 , vol. 469, # 1 p. 25 - 32
