2-氯-1-(1-萘基)乙酮合成路线 （共 10 条）
反应条件
nachfolgend Verseifen mit waessrig-methylalkoholischer Kalilauge;
参考文献
Schroeter; Mueller; Huang
Chemische Berichte, 1929 , vol. 62, p. 649
反应条件
hydrogen; Raney Ni W-4 in ethanol 0.666667 h; Ambient temperature;
参考文献
Murakami, Yasuoki; Tani, Masanobu; Tanaka, Kenjiro; Yokoyama, Yuusaku
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, p. 2023 - 2035
参考文献
Schroeter; Mueller; Huang
Chemische Berichte, 1929 , vol. 62, p. 649
反应条件
AlCl3, aluminium chloride in 1,2-dichloro-ethane
T=-5°C; 0.25 h; Inert atmosphere;
参考文献
Zhang, Yu; Stephens, David; Hernandez, Graciela; Mendoza, Rosalinda; Larionov, Oleg V.
Chemistry - A European Journal, 2012 , vol. 18, # 52 p. 16612 - 16615
反应条件
aluminium trichloride in 1,2-dichloro-ethane
T=0°C; 0.166667 h;
参考文献
Murakami, Yasuoki; Tani, Masanobu; Tanaka, Kenjiro; Yokoyama, Yuusaku
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, p. 2023 - 2035
反应条件
sulfuryl dichloride in methanol; dichloromethane
参考文献
Kisic, Andrea; Stephan, Michel; Mohar, Barbara
Organic Letters, 2013 , vol. 15, # 7 p. 1614 - 1617
反应条件
triethylamine in tetrahydrofuran
T=0°C; 96 h;
参考文献
Aoyama; Shioiri
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 11 p. 3249 - 3255
反应条件
etheric solution
anschliessend 20-stdg. Erwaermen;
参考文献
Lapkin
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 1339,1347,1348
Chem. Zentralbl., 1948 , vol. 119, p. 4978
参考文献
Lapkin
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 1339,1347,1348
Chem. Zentralbl., 1948 , vol. 119, p. 4978
反应条件
1: dimethylformamide / 1.) 0 deg C, 2 h, 2.) RT, overnight
2: NaBH4 / methanol / 0.5 h / 0 °C
View Scheme
参考文献
Walker; Wallach; Hirschfeld
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 67 - 74
