反应条件
1: 1.) LDA / 1.) THF, hexane, -10 deg C, 15 min, 2.) THF, hexane, -50 deg C, 6 h
2: Al2O3 / diethyl ether / 6 h / Ambient temperature
3: 99 percent / O2, methylene blue / methanol / 3 h / 0 °C / Irradiation
4: NaBH4, NaHCO3 / H2O / 2 h / Ambient temperature
5: p-TsOH / benzene / Heating
6: 90 percent / H2, quinoline / 5percent Pd/BaSO4 / benzene
View Scheme
参考文献
Utaka, Masanori; Kuriki, Hidesuke; Sakai, Takashi; Takeda, Akira
Journal of Organic Chemistry, 1986 , vol. 51, # 6 p. 935 - 938
