sodium perchlorate in water Electrochem. Process; prepn. by electrodeposition from aq. FeCl3 soln. (0.10 mM) and 0.1 M NaClO4 (as electrolyte) in three-electrode cell on H-terminated Si substrate potentiostatically by amperometry at const. potential of -0.8 V; Si substrate removed from cell; rinsed (water); dried in N2;
sodium perchlorate in water Electrochem. Process; prepn. by electrodeposition from aq. FeCl3 soln. (10-20 mM) and 0.1 M NaClO4 (as electrolyte) in three-electrode cell on H-terminated Si substrate potentiostatically by amperometry at const. potential of -0.8 V; Si substrate removed from cell; rinsed (water); dried in N2;