773837-37-9合成路线 (共 596 条)
反应条件
water in water aq. soln. decompd. on heating;;
参考文献
Gmelin Handbook: Na: MVol., 286, page 795 - 796
反应条件
water in water Kinetics; byproducts: NH3; at 30, 50 and 80°C;;
参考文献
Gmelin Handbook: Na: SVol.4, 4, page 1377 - 1379
反应条件
in dimethyl sulfoxide T=0 - 10°C; 3.25 h;
参考文献
HERCULES TECHNOLOGY MANAGEMENT CO V, INC.; BLAGG, Julian
Patent: WO2011/47156 A1, 2011 ;
Location in patent: Page/Page column 82 ;
WO 2011/047156 A1
反应条件
ΔnifH MoFe Inert atmosphereEnzymatic reaction;
参考文献
Lee, Chi Chung; Hu, Yilin; Ribbe, Markus W.
Proceedings of the National Academy of Sciences of the United States of America, 2012 , vol. 109, # 18 p. 6922 - 6926
反应条件
CuO in N,N-dimethyl-formamide T=100°C;
参考文献
Yapuri, Umanadh; Palle, Sadanandam; Gudaparthi, Omprakash; Narahari, Srinivasa Reddy; Rawat, Dhwajbahadur K.; Mukkanti, Khagga; Vantikommu, Jyothi
Tetrahedron Letters, 2013 , vol. 54, # 35 p. 4732 - 4734
反应条件
tri-tert-butyl phosphine; Pd2(dba)5; zinc in tetrahydrofuran; acetonitrile T=70°C; 2 h;
参考文献
Ushkov, Alexander V.; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 28 p. 10999 - 11005
反应条件
1: sodium cyanide; monosodium glutamate With sodium hydroxide in water T=97°C; Strecker Synthesis; 0.166667 h; 2: formaldehyd in water T=97°C; Strecker Synthesis; 0.5 h; 3: sodium cyanide in water T=110°C; Strecker Synthesis; 2 h;
参考文献
AKZO NOBEL CHEMICALS INTERNATIONAL B.V.; LAMMERS, Hans; HEUS, Martin; BOONSTRA, Tjerk Oedse; REICHWEIN, Adrianus Maria
Patent: WO2010/139755 A1, 2010 ;
Location in patent: Page/Page column 8-9 ;
反应条件
water; sodium hydroxide T=70°C; 8 h; Reflux; Product distribution / selectivity;
参考文献
DOW GLOBAL TECHNOLOGIES LLC.; MOORE, J. W., Jr.; BOOTH, Steven, T.; LEENHOUTS, Ray, O.
Patent: WO2011/146582 A2, 2011 ;
Location in patent: Page/Page column 10-11 ;
反应条件
in N,N-dimethyl-formamide T=100°C; 18 h; Inert atmosphere;
参考文献
GLAXOSMITHKLINE LLC; DOCK, Steven, Thomas; MCSHERRY, Allison, K.; MOORE, Michael, Lee; RIDGERS, Lance, Howard; PARRISH, Cynthia, Ann
Patent: WO2013/28445 A1, 2013 ;
Location in patent: Page/Page column 51 ;
反应条件
tetrabutylammomium bromide in dichloromethane; water T=20°C; 4 h;
参考文献
WO2013/121018 A1, ;
Page/Page column 30-31 ;