in neat (no solvent)
Irradiation (UV/VIS); mixt. of Cl2, SO2 and O2 irradiated (>320 nm) at -78°C; distd. into traps (-90, -120, -196°C); O2 pumped off; distd. intotraps (-70, -110, -196°C) by slow warming to room temp.; peroxid e from -70°C trap purified by trap-to-trap distns.; collected in -50°C trap; detd. by IR, Raman;
参考文献
Romano, Rosana M.; Vedova, Carlos O.Della; Beckers, Helmut; Willner, Helge
Inorganic Chemistry, 2009 , vol. 48, # 5 p. 1906 - 1910
Raiford
Journal of the American Chemical Society, 1914 , vol. 36, p. 675
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Raiford
American Chemical Journal, 1911 , vol. 46, p. 447
Journal of the American Chemical Society, 1914 , vol. 36, p. 673
