in neat (no solvent) byproducts: BF3; 5percent excess of OsF6 added at liquid-nitrogen temp. to B2S3, heated at 210°C for 4-6 h; volatiles determined by IR, solids did by X-ray powder diffraction;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2285 - 2288
in neat (no solvent) byproducts: BF3; 5percent excess of IrF6 added at liquid-nitrogen temp. to B2S3, heated at 210°C for 4-6 h; volatiles determined by IR, solids did by X-ray powder diffraction;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2285 - 2288
in neat (no solvent) 5percent excess of OsF6 added at liquid-nitrogen temp. to ZnS, heated at 300°C for 7-11 h; volatiles determined by IR, solids did by X-ray powder diffraction;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2285 - 2288
