(4-三氟甲基-苯基)-磷酸二乙酯合成路线 （共 6 条）
反应条件
hydrogenchloride in water 12 h; Reflux;
参考文献
Keglevich, Gyoergy; Gruen, Alajos; Boelcskei, Adrienn; Drahos, Laszlo; Kraszni, Marta; Balogh, Gyoergy T.
Heteroatom Chemistry, 2012 , vol. 23, # 6 p. 574 - 582
反应条件
α-cyclohexylcyclohexanemethanamine; triphenylphosphine; palladium diacetate in ethanol
T=76°C; 16 h;
参考文献
Goossen, Lukas J.; Dezfuli, Mohammad K.
Synlett, 2005 , # 3 art. no. G45204ST, p. 445 - 448
反应条件
palladium dichloride
T=140°C;
参考文献
GelTex Pharmaceuticals, Inc.
Patent: US2004/19020 A1, 2004 ;
Location in patent: Page/Page column 15 ;
US 20040019020 A1
反应条件
copper(I) oxide; 1,10-phenanthroline; N-ethyl-N,N-diisopropylamine in acetonitrile
T=20°C; 24 h;
参考文献
Zhuang, Rongqiang; Xu, Jian; Cai, Zhenshi; Tang, Guo; Fang, Meijuan; Zhao, Yufen
Organic Letters, 2011 , vol. 13, # 8 p. 2110 - 2113
反应条件
nickel dichloride in neat (no solvent)
T=160°C; Arbuzov Reaction; Microwave irradiation;
参考文献
Keglevich, Gyoergy; Gruen, Alajos; Boelcskei, Adrienn; Drahos, Laszlo; Kraszni, Marta; Balogh, Gyoergy T.
Heteroatom Chemistry, 2012 , vol. 23, # 6 p. 574 - 582
反应条件
hydrogenchloride; magnesium in diethyl ether
-76 deg C, 1.5 h, RT, 1.5 h;
参考文献
Grabiak, Raymond C.; Miles, James A.; Schwenzer, Gretchen M.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 9, p. 197 - 202
