tetrahydrofuran in tetrahydrofuran B4H10 dissolved in THF at -80°C, kept at 0°C for 4 h, treated with PH3 at -60°C, allowed to warm to 0°C, stored for67 h; NMR anal.;
in acetonitrile Kinetics; continnous-flow apparatus, passge of PH3/Ar mixt.; gas chrommatographie anal.;
参考文献
Dorfman, Ya. A.; Levina, L. V.; Petrova, T. V.; Emel'yanova, V. S.; Polimbetova, G. S.
Journal of General Chemistry USSR (English Translation), 1989 , vol. 59, p. 1292 - 1293
Zhurnal Obshchei Khimii, 1989 , vol. 59, p. 1454 - 1455
