in neat (no solvent) dry mixture of 2mol AgCH3CO2 and 1mol I2 (in mixture with powdered porcelain), on heating to 130-140°C for a longer period of time;;
参考文献
Simonini, A.
Monatshefte fuer Chemie, 1892 , vol. 13, p. 320 - 325
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Gmelin Handbook: Ag: MVol.B5, 2.2.7.3, page 126 - 127
in methanol byproducts: C2H4, CO2; Electrolysis; electrolysis of 3 percent soln. of NaCH3CO2 in methanol using polished Pt sheet as anode, no formation of O, HCO2H or CH2O, yield of C2H6 does not depend on temperature;;