联苯-4,4-二羧酸二甲酯合成路线 （共 64 条）
反应条件
trifluoroacetic acid; cobalt(II) dibromide; zinc dibromide in acetonitrile the mixt. in CH3CN was stirred at room temp., then arylbromide was added, stirred at room temp.; GC analysis;
参考文献
Journal of the American Chemical Society, , vol. 125, # 13 p. 3867 - 3870
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
反应条件
palladium on activated charcoal in m-xylene T=140°C; 12 h;
参考文献
Matsushita; Sakamoto; Murakami; Matsui
Synthetic Communications, 1994 , vol. 24, # 22 p. 3307 - 3313
反应条件
1: aq. K3PO4 / toluene / 1 h 2: 21 percent / Mg; methanol / Pd/C / 24 h / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 13, # 5 p. 1432 - 1441
反应条件
NiCl2((PPh3)P)2; tetraethylammonium iodide; zinc in tetrahydrofuran 1.) r.t., 5 min, 2.) 67 deg C, 5 h;
参考文献
Percec, Virgil; Bae, Jin-Young; Zhao, Mingyang; Hill, Dale H.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 176 - 185
反应条件
potassium cyanide T=20°C; 24 h;
参考文献
Ahn, Jung-Mo; Wentworth Jr., Paul; Janda, Kim D
Chemical communications (Cambridge, England), 2003 , # 4 p. 480 - 481
反应条件
NiCl2((PPh3)P)2; tetraethylammonium iodide; zinc in tetrahydrofuran 1.) r.t, 5 min, 2.) 67 deg C, 5 h;
参考文献
Percec, Virgil; Bae, Jin-Young; Zhao, Mingyang; Hill, Dale H.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 176 - 185
反应条件
tetraethylammonium iodide; zinc; NiCl2((PPh3)P)2 in tetrahydrofuran T=67°C; 24 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 21 p. 6895 - 6903
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
bis(η3-allyl-μ-chloropalladium(II)); potassium acetate in N,N-dimethyl acetamide T=120°C; 12 h; Inert atmosphere;
参考文献
Gottumukkala, Aditya L.; Doucet, Henri
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 14-15 p. 2183 - 2188
