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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
肌酸酐
合成路线
（共 23 条）
79617-96-2
舍曲林
→
反应条件
79559-97-0
肌酸酐
反应条件
hydrogenchloride in propan-1-ol T=30°C; 1 h; Product distribution / selectivity;
参考文献
RECORDATI SA
Patent: WO2005/12224 A1, 2005 ;
Location in patent: Page/Page column 7 ;
244223-89-0
→
反应条件
79559-97-0
肌酸酐
反应条件
sodium hydroxide in dichloromethane; water Industrial scale;
参考文献
Vukics, Krisztina; Fodor, Tamas; Fischer, Janos; Fellegvari, Iren; Levai, Sandor
Organic Process Research and Development, 2002 , vol. 6, # 1 p. 82 - 85
267884-85-5
→
反应条件
79559-97-0
肌酸酐
反应条件
hydrogenchloride in ethyl acetate T=20°C; 6 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Chen, Fei; Ding, Ziyuan; He, Yanmei; Qin, Jie; Wang, Tianli; Fan, Qing-Hua
Tetrahedron, 2012 , vol. 68, # 26 p. 5248 - 5257
836597-67-2
→
反应条件
79559-97-0
肌酸酐
反应条件
hydrogenchloride in acetonitrile T=20°C; 1 h; Product distribution / selectivity;
参考文献
RECORDATI SA
Patent: WO2005/12224 A1, 2005 ;
Location in patent: Page/Page column 10 ;
928057-23-2
→
反应条件
79559-97-0
肌酸酐
反应条件
hydrogenchloride in diethyl ether; nitromethane T=25 - 30°C; 1 h; Product distribution / selectivity;
参考文献
Kintali, Ramana Venkata; Ludescher, Johannes; Nair, Raji; Sawant, Sudhir
Patent: US2007/54960 A1, 2007 ;
Location in patent: Page/Page column 2 ;
64-19-7
醋酸
+
79617-96-2
舍曲林
→
反应条件
79559-97-0
肌酸酐
反应条件
1: in water T=5 - 25°C; 1.33333 h; 2: With hydrogenchloride in water T=5 - 15°C; 1.25 h;
参考文献
WO2005/47229 A2, ;
Page/Page column 7 ;
WO 2005/047229 A2
928057-20-9
→
反应条件
79559-97-0
肌酸酐
反应条件
hydrogenchloride in diethyl ether; isobutyl methylketone T=25 - 70°C; 3 h; Product distribution / selectivity;
参考文献
Kintali, Ramana Venkata; Ludescher, Johannes; Nair, Raji; Sawant, Sudhir
Patent: US2007/54960 A1, 2007 ;
Location in patent: Page/Page column 2 ;
928057-24-3
→
反应条件
79559-97-0
肌酸酐
反应条件
hydrogenchloride in diethyl ether; nitromethane T=25 - 30°C; 1 h; Product distribution / selectivity;
参考文献
Kintali, Ramana Venkata; Ludescher, Johannes; Nair, Raji; Sawant, Sudhir
Patent: US2007/54960 A1, 2007 ;
Location in patent: Page/Page column 2 ;
928057-22-1
→
反应条件
79559-97-0
肌酸酐
反应条件
hydrogenchloride in diethyl ether; nitromethane T=25 - 30°C; 1 h; Product distribution / selectivity;
参考文献
Kintali, Ramana Venkata; Ludescher, Johannes; Nair, Raji; Sawant, Sudhir
Patent: US2007/54960 A1, 2007 ;
Location in patent: Page/Page column 2 ;
79560-20-6
萘亚胺
→
反应条件
反应条件
1: With hydrogen; pyridine hydrochloride; 50 Pd/C in methanol T=25 - 35°C; 6 h; 2: With hydrogenchloride in methanol; water pH=1 - 2; Product distribution / selectivity;
参考文献
WO2007/71421 A1, ;
Page/Page column 4 ;
1
2
3
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