80937-33-3合成路线 (共 1249 条)
反应条件
nitric acid; sodium nitrate; Titanium(IV) oxide in not given Kinetics; 413 - 1073 K;
参考文献
Liu; Li; Che; Lei
Journal of thermal analysis, 1995 , vol. 45, # 1-2 p. 39 - 46
反应条件
in neat (no solvent) powdered Na2Sforms at ambient temperature with air or O2 in presense of highly dispersed charcoal Na2S2O3;; mixture is extracted with H2O, formation of Na2S2O3*5H2O on concentrating, or removal of NaOH via extraction with alcohol;;
参考文献
Naef
J. Soc. Chem. Ind., London, Abstr., 1922 , vol. 41, p. 215 - 215
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Gmelin Handbook: Na: MVol., 210, page 607 - 609
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Naef
Patent: EP174653 , 1920 ;
反应条件
in water dissolving 80g KI and 40g KOH in 500ml H2O; 24h at 250°C with O2 pressure of 90 - 100 atm;; product mixture;;
参考文献
Z. Anorg. Chem., , vol. 188, p. 140 - 140
反应条件
potassium hydroxide in water at 250°C at 90-100 atm. O2-pressure; in strongly alkaline KOH soln.;;
参考文献
Gmelin Handbook: I: MVol.2, 132, page 533 - 535
反应条件
in neat (no solvent) Irradiation (UV/VIS); mixt. of Cl2, SO2 and O2 irradiated (>320 nm) at -78°C; distd. into traps (-90, -120, -196°C); O2 pumped off; distd. intotraps (-70, -110, -196°C) by slow warming to room temp.; peroxid e from -70°C trap purified by trap-to-trap distns.; collected in -50°C trap; detd. by IR, Raman;
参考文献
Romano, Rosana M.; Vedova, Carlos O.Della; Beckers, Helmut; Willner, Helge
Inorganic Chemistry, 2009 , vol. 48, # 5 p. 1906 - 1910
反应条件
iron powder in water reduction of O2 with Fe(2+) in presence of EDTA and ascorbic acid;;
参考文献
Kajihara, Koichi; Hirano, Masahiro; Skuja, Linards; Hosono, Hideo
Journal of the American Chemical Society, 2006 , vol. 128, # 16 p. 5371 - 5374
反应条件
in gaseous matrix Kinetics; H and O2 reacted in excess of Ar in fast flow-discharge tube at 2-10 Torr and at 231-512 K; detected by mass spectrometry and GC chromy;
参考文献
Hanning-Lee, Mark A.; Pilling, Michael J.; Warr, Jonathan F.
Journal of the Chemical Society, Faraday Transactions, 1991 , vol. 87, # 18 p. 2907 - 2912
反应条件
in neat (no solvent) byproducts: OH, H2O2, H2O; a streaming mixture of H2 and He heated to 1000 °C was mixed with O2;; mass spectroscopy;;
参考文献
Johnson, T. J.; Wienhold, F. G.; Burrows, J. P.; Harris, G. W.; Burkhard, H.
Journal of Physical Chemistry, 1991 , vol. 95, # 17 p. 6499 - 6502
反应条件
in neat (no solvent) Kinetics; byproducts: C2H4, C2H5O2; Irradiation (UV/VIS); reaction of O2 with C2H5 radicals formed by flash-light photolysis (22 °C, 5-100 Torr total pressure); 99.9percent of C2H5 reacted with formation of C2H5O2; rate constant;;
参考文献
Dingledy; Calvert
Journal of the American Chemical Society, 1963 , vol. 85, p. 856
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Benson, S. W.
J. Am. Chem. Soc. (Fussnote), 1965 , vol. 87, p. 972 - 979
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Gmelin Handbook: O: MVol.8, 35, page 2605 - 2607
反应条件
chlorine; nitrogen(IV) oxide in gas byproducts: HCl, CH2O; Irradiation (UV/VIS); flash photolysis of a mixt. of Cl2, CH3OH, O2, and NO2;; not isolated, detected by UV spectroscopy;;
参考文献
Lightfoot, P. D.; Veyret, B.; Lesclaux, R.
Journal of Physical Chemistry, 1990 , vol. 94, # 2 p. 708 - 714