80937-33-3合成路线 （共 1249 条）
参考文献
US2004/15014 A1, ;
Page 11-12 ;
反应条件
N2 in neat (no solvent, gas phase) Kinetics; reaction over temp. range of 350-624 K in presence of N2 by static-flow reaction; detected by laser pulse / probe technique;
参考文献
Journal of Physical Chemistry, , vol. 97, # 24 p. 6449 - 6456
反应条件
in neat (no solvent) byproducts: MgO3; codeposition of pulsed laser evaporated Mg atoms with O2 in excess Ar on 10 K substrate; mechanism discussed; not isolated, detn. by IR;
参考文献
Journal of Physical Chemistry, , vol. 97, # 49 p. 12700 - 12704
反应条件
in neat (no solvent) byproducts: C3H6ClCCl3, C3H6O; 20°C, 96 h; further products;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 50, p. 454 - 462
Zhurnal Obshchei Khimii, , vol. 50, p. 567 - 575
反应条件
in perchloric acid; acetonitrile Kinetics; 298 K; not isolated, UV/VIS monitoring (600 - 700nm);
参考文献
Inorganic Chemistry, , vol. 28, p. 2459 - 2465
反应条件
in water dissolving 80g KI and 40g KOH in 1000ml H2O; 48h at 250°C with O2 pressure of 90 - 100 atm;;
参考文献
Gmelin Handbook: I: MVol.2, 120, page 504 - 506
反应条件
in water dissolving 80g KI and 40g KOH in 500ml H2O; 24h at 250°C with O2 pressure of 90 - 100 atm;; product mixture;;
参考文献
Z. Anorg. Chem., , vol. 188, p. 140 - 140
反应条件
in neat (no solvent) at temp. above 600°C and pressures higher than 100atm;;
参考文献
Henglein, F. A.; Teichmann, L.
Z. Anorg. Chem., 1930 , vol. 188, p. 138 - 138
反应条件
potassium hydroxide in water at 250°C at 90-100 atm. O2-pressure; in strongly alkaline KOH soln.;;
参考文献
Gmelin Handbook: I: MVol.2, 132, page 533 - 535
反应条件
in neat (no solvent) heating dry equivalent mixture of KClO3 and KI to temp. between melting point of KClO3 and decomposition temp. of KIO3 in stream of O2; cooling down;; trituration and washing with cold H2O, fractionated crystallization;;
参考文献
Gmelin Handbook: I: MVol.2, 121, page 506 - 508
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Stas, J. S.
Nouvelles recherches sur les lois des proportions chimiques, sur les poids atomiques et leurs rapports mutuels, Bruxelles 1865, S. 113
