1: anhydrous propionitrile With lithium diisopropyl amide in tetrahydrofuran; hexane; cyclohexane T=-78°C; 0.25 h; Inert atmosphere; 2: diethyl chlorophosphate in tetrahydrofuran; hexane; cyclohexane T=-78 - 20°C; 1.16667 h; Inert atmosphere;
参考文献
Sovdat, Tina; Bassolino, Giovanni; Liebel, Matz; Schnedermann, Christoph; Fletcher, Stephen P.; Kukura, Philipp
Journal of the American Chemical Society, 2012 , vol. 134, # 20 p. 8318 - 8320
Farbenfabr. Bayer
Patent: DE814152 , 1948 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Schrader
Angewandte Chemie, Monogr. 62 <1952> 48
Full Text Show Details
Schrader; Bios
Final Rep., p. 714 Item 8 S. 52