in diethyl ether; benzene byproducts: LiCl; addn. of SnCl4 in benzene under of air and moisture to a soln. of LiN(C2H5)2 in ether; reflux for 4 h; filtration;; solvent distd. off; distn. of the residue in high vac.;;
参考文献
Jones, K.; Lappert, M. F.
Journal of the Chemical Society, 1965 , p. 1944 - 1951
Sauer et al.
Chemische Berichte, 1958 , vol. 91, p. 1461,1472
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Gilman et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 2106