2-羟基-1,4-萘醌合成路线 (共 313 条)
反应条件
ethanol; n-dodecylamine hydrochloride
anschliessendes Behandeln mit wss.Formaldehyd;
参考文献
Dalgliesh
Journal of the American Chemical Society, 1949 , vol. 71, p. 1697,1700
反应条件
lithium hydride in dimethyl sulfoxide
45 deg C, 5 h; 25 deg C, 10 h;
参考文献
Sun, Jerry S.; Geiser, Andrew H.; Frydman, Benjamin
Tetrahedron Letters, 1998 , vol. 39, # 45 p. 8221 - 8224
反应条件
potassium carbonate in acetone
1 h; Reflux;
参考文献
Epifano, Francesco; Genovese, Salvatore; James Squires; Gray, Matthew A.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 9 p. 3130 - 3135
反应条件
triphenylphosphine in tetrahydrofuran
参考文献
BTG International Limited
Patent: US5962002 A1, 1999 ;
反应条件
(i) SOCl2, (ii) aq. H2O2, Py, (iii) /BRN= 1565260/; Multistep reaction;
参考文献
Bullock
Journal of medicinal chemistry, 1968 , vol. 11, # 3 p. 419 - 424
反应条件
1: 80 percent / ethylenediamine diacetate / benzene / 5 h / Heating
2: 99 percent / H2 / Pd/C / ethyl acetate / 0.33 h / 517.15 Torr
View Scheme
参考文献
Yong, Rok Lee; Won, Kyong Lee
Synthetic Communications, 2004 , vol. 34, # 24 p. 4537 - 4543
反应条件
in 1,4-dioxane
Knoevenagel condensation; Reflux;
参考文献
Ferreira, Sabrina Baptista; Kaiser, Carlos Roland; Ferreira, Vitor Francisco
Organic Preparations and Procedures International, 2009 , vol. 41, # 3 p. 211 - 215
反应条件
formic acid in ethanol; water
T=200°C; P=155.149 - 155149 Torr; 3 h; chemoselective reaction;
参考文献
Ferreira, Sabrina Baptista; Rodriguesdarocha, David; Carneiro, Jose Walkimar M.; Santos, Wilson Costa; Ferreira, Vitor Francisco
Synlett, 2011 , # 11 p. 1551 - 1554
反应条件
copper(II) sulfate
T=50°C; 2.5 h;
参考文献
Bansal; Thapliyal; Khanna
Synthetic Communications, 1995 , vol. 25, # 11 p. 1669 - 1675
参考文献
Syntex (U.S.A.) Inc.
Patent: US5091558 A1, 1992 ;