L-(+)-酒石酸二乙酯合成路线 (共 47 条)
参考文献
Patterson; Todd
Journal of the Chemical Society, 1929 , p. 1769
反应条件
toluene-4-sulfonic acid in benzene 8 h; RefluxInert atmosphereDean-Stark;
参考文献
Zou, Liwei; Wang, Baomin; Mu, Hongfang; Zhang, Huanrui; Song, Yuming; Qu, Jingping
Organic Letters, 2013 , vol. 15, # 12 p. 3106 - 3109
反应条件
hydrazine in ethanol; water Heating / reflux;
参考文献
FIRMENICH SA; UNIVERSITE LOUIS PASTEUR; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
Patent: WO2006/16248 A1, 2006 ;
Location in patent: Page/Page column 19 ;
反应条件
1: With 4 A molecular sieve; toluene-4-sulfonic acid in dichloromethane 168 h; Heating; 2: With lithium aluminium tetrahydride in tetrahydrofuran 5 h; Heating; Further stages.;
参考文献
Kwong, Joey S.W.; Mahon, Mary F.; Lloyd, Matthew D.; Threadgill, Michael D.
Tetrahedron, 2007 , vol. 63, # 51 p. 12601 - 12607
反应条件
sodium periodate in dichloromethane; water Heating;
参考文献
Bailey, Patrick D; Smith, Peter D; Pederson, Frederick; Clegg, William; Rosair, Georgina M; Teat, Simon J
Tetrahedron Letters, 2002 , vol. 43, # 6 p. 1067 - 1070
反应条件
T=18°C; Geschwindigkeit;
参考文献
Criegee
Chemische Berichte, 1931 , vol. 64, p. 260,262, 265
Chemische Berichte, 1932 , vol. 65, p. 1770
反应条件
1: With titanium(IV) isopropylate; 4 A molecular sieve in dichloromethane T=-20°C; 0.5 h; 2: With tert.-butylhydroperoxide in decane; dichloromethane T=-20°C; 68 h; Further byproducts given;
参考文献
Paju, Anne; Kanger, Tonis; Pehk, Tonis; Lindmaa, Rasmus; Mueuerisepp, Aleksander-Mati; Lopp, Margus
Tetrahedron Asymmetry, 2003 , vol. 14, # 11 p. 1565 - 1573
反应条件
sodium tetrahydroborate in ethanol 1.) r.t., 12 h, 2.) reflux, 8 h;
参考文献
Terfort
Synthesis, 1992 , # 10 p. 951 - 953
反应条件
T=100 - 165°C; unter Hochdruck.Hydrogenation;
参考文献
Adkins; Billica
Journal of the American Chemical Society, 1948 , vol. 70, p. 3121
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Trenner; Bacher
Journal of the American Chemical Society, 1949 , vol. 71, p. 2353
反应条件
indium; iodine transesterification; 7 h; Heating;
参考文献
Ranu, Brindaban C.; Dutta, Pinak; Sarkar, Arunkanti
Journal of Organic Chemistry, 1998 , vol. 63, # 17 p. 6027 - 6028