n-butyllithium in tetrahydrofuran; hexane T=-60°C; Flow reactor;
参考文献
Newby, James A.; Huck, Lena; Blaylock, D. Wayne; Witt, Paul M.; Ley, Steven V.; Browne, Duncan L.
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 263 - 271
3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide in acetonitrile Zn dust (1.5 equiv., acid-activated) , CoBr2 (0.1 equiv.), stirred for 5min with allyl chloride (0.3 equiv.), a soln. of aryl halide (1 equiv.) and a soln. 1 equiv. of B compd. added at room temp., stirred for 30 mi n, tranesterificated with pinacol; hydrolized (NH4Cl), extd. (diethyl ether);
参考文献
Claudel, Stephanie; Gosmini, Corinne; Paris, Jean Marc; Perichon, Jacques
Chemical Communications, 2007 , # 35 p. 3667 - 3669
