2,4,6-三硝基氯苯合成路线 （共 249 条）
反应条件
tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
T=20°C; Arbuzov reaction; Inert atmosphereElectrolysis;
参考文献
Cruz, Hugo; Gallardo, Iluminada; Guirado, Gonzalo
European Journal of Organic Chemistry, 2011 , # 36 p. 7378 - 7389
反应条件
1: tetra-n-butylammonium tetrafluoroborate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere; Electrolysis
2: tetra-n-butylammonium tetrafluoroborate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere; Electrolysis
View Scheme
参考文献
Cruz, Hugo; Gallardo, Iluminada; Guirado, Gonzalo
European Journal of Organic Chemistry, 2011 , # 36 p. 7378 - 7389
反应条件
ethanol; hydrazine hydrate
参考文献
Curtius; Dedichen
Journal fuer Praktische Chemie (Leipzig), 1894 , vol. <2> 50, p. 254
Journal fuer Praktische Chemie (Leipzig), 1895 , vol. <2> 52, p. 272
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Purgotti
Gazzetta Chimica Italiana, 1894 , vol. 24 I, p. 113
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Borsche
Chemische Berichte, 1921 , vol. 54, p. 1288
参考文献
Allen
Organic Syntheses, 1933 , vol. 13, p. 37
Organic Syntheses, 1943 , vol. Coll. Vol. II, p. 229
参考文献
Curtius; Dedichen
Journal fuer Praktische Chemie (Leipzig), 1894 , vol. <2> 50, p. 254
Journal fuer Praktische Chemie (Leipzig), 1895 , vol. <2> 52, p. 272
Full Text Show Details
Purgotti
Gazzetta Chimica Italiana, 1894 , vol. 24 I, p. 113
反应条件
1: 69 percent / aq. ethanol / 3 h / Heating
2: 51 percent / acetic acid
View Scheme
参考文献
Vichard, Dominique; Boubaker, Taoufik; Terrier, Francois; Pouet, Marie-Jose; Dust, Julian M.; Buncel, Erwin
Canadian Journal of Chemistry, 2001 , vol. 79, # 11 p. 1617 - 1623
参考文献
Emokpae, Thomas A.; Atasie, Nkechi V.
International Journal of Chemical Kinetics, 2005 , vol. 37, # 12 p. 744 - 750
参考文献
Cerniani et al.
Bollettino Scientifico della Facolta di Chimica Industriale di Bologna, 1954 , vol. 12, p. 114,123
反应条件
in dimethyl sulfoxide
参考文献
Sekiguchi, Shizen; Ishikura, Hiromi; Hirosawa, Yukitoshi; Ono, Nobuyuki
Tetrahedron, 1990 , vol. 46, # 16 p. 5567 - 5578
反应条件
1: 100 percent / diethyl ether / Ambient temperature
2: 64.3 percent / acetonitrile / 24 h / Ambient temperature
View Scheme
参考文献
Vizgert, R. V.; Sheiko, S. G.; Kulishova, T. P.; Pekhtereva, T. M.; Nardekova, V. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 166 - 169
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 1 p. 185 - 189
