pinacol borane; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in tetrahydrofuran byproducts: H2; CH3OC6H4OH reacted with (C2H5)2SiH2 and Ir complex in C6H6, reacted withB compds., Ir complex and 4,4'-di-tert-butylpyridine in THF at 80.degre e.C, reacted with aq. KHF2 in THF; obtained contaminated;
参考文献
Boebel, Timothy A.; Hartwig, John F.
Journal of the American Chemical Society, 2008 , vol. 130, # 24 p. 7534 - 7535
1: 36 percent / NaH; CuBr*SMe2 / dimethylformamide / 3 h / Heating 2: 94 percent / H2 / Pd/C / methanol / 3 h / 20 °C View Scheme
参考文献
De La Fuente, Jesus Angel; Manzanaro, Sonia; Martin, Maria Jesus; De Quesada, Teresa G.; Reymundo, Isabel; Luengo, Santos M.; Gago, Federico
Journal of Medicinal Chemistry, 2003 , vol. 46, # 24 p. 5208 - 5221
