908094-04-2合成路线 (共 238 条)
反应条件
T=-196°C; (photolysis);
参考文献
Journal of the American Chemical Society, , vol. 101, p. 6009 - 6012
反应条件
in solid matrix T=-110°C; Irradiationtemperature dependence of product distributions, added sensitizer; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 104, # 11 p. 3156 - 3162
反应条件
Ambient temperatureIrradiationrelative yields of products for different substituents;
参考文献
Tetrahedron, , vol. 41, # 8 p. 1435 - 1440
反应条件
in 1,2-dichloro-ethane T=20°C; 1 h; Further byproducts given. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 3 p. 726 - 730
反应条件
in tetrahydrofuran (Ar), Schlenk techniques; slow addn. of soln. of N compd. in THF to soln. of Rh complex in THF at room temp.;
参考文献
Palacios, Laura; Miao, Xiaowei; Di Giuseppe, Andrea; Pascal, Simon; Cunchillos, Carmen; Castarlenas, Ricardo; Perez-Torrente, Jesus J.; Lahoz, Fernando J.; Dixneuf, Pierre H.; Oro, Luis A.
Organometallics, 2011 , vol. 30, # 19 p. 5208 - 5213
反应条件
tin(ll) chloride in methanol; dichloromethane 48 h; Ambient temperature;
参考文献
Chittenden, Gordon J. F.
Carbohydrate Research, 1981 , vol. 91, p. 85 - 88
反应条件
in tetrahydrofuran T=0°C; 3 h; Title compound not separated from byproducts;
参考文献
Huisgen, Rolf; Xingya, Li
Heterocycles, 1983 , vol. 20, # 12 p. 2363 - 2368
反应条件
T=-196°C; Irradiation; Further byproducts given;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Chemistry Letters, 1980 , p. 293 - 296
反应条件
T=15°C; Irradiationvariation of temperature, matrix effect, further chloro compound; Product distribution;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Chemistry Letters, 1980 , p. 293 - 296
反应条件
1: cycloheptanone With scandium tris(trifluoromethanesulfonate) in toluene T=-78 - 20°C; Inert atmosphere; 2: phenyldiazomethane in toluene T=0°C; 1 h; Inert atmosphere;
参考文献
Rendina, Victor L.; Moebius, David C.; Kingsbury, Jason S.
Organic Letters, 2011 , vol. 13, # 8 p. 2004 - 2007