908094-04-2合成路线 （共 238 条）
反应条件
in tetrahydrofuran
T=20°C; 1 h;
参考文献
Oshima, Takumi; Nagai, Toshikazu
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 3 p. 726 - 730
反应条件
in methanol
T=20°C; 1 h; Further byproducts given;
参考文献
Oshima, Takumi; Nagai, Toshikazu
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 3 p. 726 - 730
反应条件
in various solvent(s)
T=20°C; 1 h;
参考文献
Oshima, Takumi; Nagai, Toshikazu
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 3 p. 726 - 730
反应条件
1: With triethylamine in diethyl ether
T=0°C; Acylation; Heating;
2: With silica gel
Cyclization; aromatization;
参考文献
Ghosh, Somnath; Banerjee, Indira; Baul, Susmita
Tetrahedron, 1999 , vol. 55, # 38 p. 11537 - 11546
反应条件
scandium tris(trifluoromethanesulfonate) in toluene
T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Wommack, Andrew J.; Moebius, David C.; Travis, Austin L.; Kingsbury, Jason S.
Organic Letters, 2009 , vol. 11, # 15 p. 3202 - 3205
反应条件
lithium bromide in diethyl ether
T=0°C;
参考文献
Loeschorn, Carol A.; Nakajima, Masayuki; Anselme, Jean-Pierre
Bulletin des Societes Chimiques Belges, 1981 , vol. 90, # 9 p. 985 - 986
反应条件
tetrafluoroboric acid in dichloromethane
T=-40°C; 0.416667 h;
参考文献
Liotta, Louis J.; Ganem, Bruce
Israel Journal of Chemistry, 1991 , vol. 31, # 3 p. 215 - 222
反应条件
benzophenone
0.25 h; Irradiation; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Creary, Xavier
Journal of the American Chemical Society, 1980 , vol. 102, # 5 p. 1611 - 1618
反应条件
1: cyclohexanone With scandium tris(trifluoromethanesulfonate) in toluene
T=20°C; 0.0833333 h; Inert atmosphere;
2: phenyldiazomethane in toluene
T=-78 - 0°C; Inert atmosphere;
参考文献
Rendina, Victor L.; Kaplan, Hilan Z.; Kingsbury, Jason S.
Synthesis, 2012 , vol. 44, # 5 p. 686 - 693
反应条件
disulfur dichloride; triethylamine in dichloromethane
T=0 - 5°C; 2 h;
参考文献
Okuma, Kentaro; Nagakura, Kazuko; Nakajima, Yasutaka; Kubo, Kento; Shioji, Kosei
Synthesis, 2004 , # 12 p. 1929 - 1931
