反应条件
AlCl3; Al; H2O2 in 2-methyl cyclohexane (N2); addn. of methylcyclohexane to a mixt. of ligand, ferrocene, AlCl3,Al, heating to 30°C, addn. of TiCl4, heating to 90°C, sti rring for 3 h, addn. of aq. HCl, addn. of aq. H2O2, stirring, addn. of aq. KPF6, cooling to 0°C; filtration, evapn., recrystn. (acetone);
参考文献
Kuendig, E. Peter; Jeger, Patrick; Bernardinelli, Gerald
Inorganica Chimica Acta, 2004 , vol. 357, # 6 p. 1909 - 1919
