Yamamoto, Yoshinori; Yamamoto, Shinichi; Yatagai, Hidetaka; Maruyama, Kazuhiro
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2318 - 2325
copper(l) iodide; boron trifluoride diethyl etherate in tetrahydrofuran
other Lewis acids, solvents; Product distribution;
参考文献
Yamamoto, Yoshinori; Yamamoto, Shinichi; Yatagai, Hidetaka; Maruyama, Kazuhiro
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2318 - 2325
methanesulfonic acid in tetrahydrofuran
dropwise addn. of CH3Li (1 equiv.) to soln. of C6H11B(OC2(CH3)4O) (2.5 mmol) in THF at -78°C via syringe; stirring at -78°C for 3 h; addn. of CH3SO3H at -78°C; warming slowly to room temp.; stirring at room temp.;; not isolated; product distribution is determined by 11B-NMR;;
参考文献
Brown, Herbert C.; Vasumathi, Nagarajan; Joshi, Navalkishore N.
Organometallics, 1993 , vol. 12, p. 1058 - 1067
