1-苯基-1,3-丁二酮合成路线 (共 471 条)
反应条件
boron trifluoride diethyl etherate in n-heptane; benzene 2 h; Ambient temperaturealso with benzylideneacetone;
参考文献
Ahmad, Mesbah U.; Rashid, Muhammad A.; Mullah, Khairuzzaman B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 266 - 267
参考文献
Texier-Boullet, F.; Klein, B.; Hamelin, J.
Synthesis, 1986 , # 5 p. 409 - 411
反应条件
Product distribution;
参考文献
v. Auwers; Stuhlmann
Chemische Berichte, 1926 , vol. 59, p. 1054
参考文献
ORIENT CHEMICAL INDUSTRIES, LTD.
Patent: EP1862860 A1, 2007 ;
反应条件
aluminum oxide; hydrazine hydrate T=20°C; 1 h;
参考文献
Synthesis, , # 5 p. 409 - 411
反应条件
hydrazine in methanol T=13°C; Rate constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 7 p. 1361 - 1364
Zhurnal Organicheskoi Khimii, , vol. 20, # 7 p. 1494 - 1497
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal 1.) baker's yeast; 2.) aq. EtOH, 24 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Bracher; Litz
Archiv der Pharmazie, 1994 , vol. 327, # 9 p. 591 - 593
反应条件
triethylamine T=20°C; 0.583333 h;
参考文献
Aizpurua, Jesus Mari; Palomo, Claudio
Synthesis, 1982 , # 4 p. 280 - 281
反应条件
toluene-4-sulfonic acid in benzene 8 h; Heating;
参考文献
Tarzia; Panzone; Leali; Burdisso; Schiatti; Selva
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 6 p. 538 - 558
反应条件
sodium hydrogencarbonate 1) EtOH, rt, 10 min, 2) toluene, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Abdalla; Sowell Sr.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1201 - 1207