1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
sodium tetrahydroborate; sodium hydride; nickel dichloride 1) THF, room temperature, 2) MeOH, ice cooling; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Wang, Feng; Chiba, Kazuhiro; Tada, Masahiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 15 p. 1897 - 1900
参考文献
Bauer
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1912 , vol. 154, p. 1093
参考文献
McElvain; Weber
Journal of the American Chemical Society, 1941 , vol. 63, p. 2192,2193
反应条件
carbon monoxide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; selenium in tetrahydrofuran T=120°C; P=22800 Torr; 24 h;
参考文献
Tetrahedron Letters, , vol. 33, # 42 p. 6347 - 6350
反应条件
potassium fluoride; palladium diacetate; chlorobenzene in tetrahydrofuran; water T=20°C; 1 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 4 p. 584 - 587
反应条件
nickel T=200°C; Hydrogenation;
参考文献
Sabatier; Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1907 , vol. 145, p. 1127
Annales de Chimie (Cachan, France), 1909 , vol. <8> 16, p. 86
反应条件
T=125°C; P=91938.4 - 147102 Torr; Hydrogenation;
参考文献
Sprague; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 2669,2671
反应条件
T=200°C; Hydrogenation;
参考文献
Sabatier; Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1907 , vol. 145, p. 1127
Annales de Chimie (Cachan, France), 1909 , vol. <8> 16, p. 86
反应条件
water; toluene-4-sulfonic acid in acetonitrile T=80°C; 16 h; Sealed tube;
参考文献
Organic Letters, , vol. 16, # 3 p. 764 - 767
反应条件
in methanol T=20°C; Cyclization; Condensation; 6 h;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 54, # 7 p. 881 - 886
