3,4-环氧-1-丁烯合成路线 (共 241 条)
参考文献
Freedman; Becker
Journal of Organic Chemistry, 1951 , vol. 16, p. 1701,1708
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide
ambient temp.; product yield: 77percent, ratio 1,4- : 1,2-product = 87:13; ratio E:Z = 10:1;
参考文献
Echavarren, Antonio M.; Tueting, David R.; Stille, J. K.
Journal of the American Chemical Society, 1988 , vol. 110, p. 4039 - 4041
反应条件
water; dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide
12 h; Yield given;
参考文献
Tueting, David R.; Echavarren, Antonio M.; Stille, J. K.
Tetrahedron, 1989 , vol. 45, # 4 p. 979 - 992
参考文献
Yamaguchi, Ryohei; Hamasaki, Takashi; Sasaki, Tohru; Ohta, Tetsuo; Utimoto, Kiitiro; et al.
Journal of Organic Chemistry, 1993 , vol. 58, # 5 p. 1136 - 1143
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-65°C; 6 h;
参考文献
Fedorov, Alexey; Fu, Changchun; Linden, Anthony; Heimgartner, Heinz
European Journal of Organic Chemistry, 2005 , # 8 p. 1613 - 1619
参考文献
Culvenor; Davies; Heath
Journal of the Chemical Society, 1949 , p. 278,281
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide
ambient temp.; product yield: 83percent, ratio 1,4- : 1,2-product = 88:12; 1,4-product: ratio E:Z = 18:1;
参考文献
Echavarren, Antonio M.; Tueting, David R.; Stille, J. K.
Journal of the American Chemical Society, 1988 , vol. 110, p. 4039 - 4041
反应条件
water; dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide
12 h; Yield given;
参考文献
Tueting, David R.; Echavarren, Antonio M.; Stille, J. K.
Tetrahedron, 1989 , vol. 45, # 4 p. 979 - 992
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenylphosphine in benzene
T=40°C; Yield given. Yields of byproduct given;
参考文献
Matsuhashi, Hayao; Asai, Satoshi; Hirabayashi, Kazunori; Hatanaka, Yasuo; Mori, Atsunori; Hiyama, Tamejiro
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 8 p. 1943 - 1952
反应条件
caesium carbonate; palladium-pincer in tetrahydrofuran
T=0°C; Suzuki-Miyaura cross-coupling; 16 h; Product distribution; Further Variations:Catalysts;
参考文献
Kjellgren, Johan; Aydin, Juhanes; Wallner, Olov A.; Saltanova, Irina V.; Szabo, Kalman J.
Chemistry - A European Journal, 2005 , vol. 11, # 18 p. 5260 - 5268