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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
93026-61-0
合成路线
（共 10 条）
290825-97-7
+
100-46-9
苄胺
→
反应条件
93026-61-0
反应条件
triphenylphosphine; silver trifluoromethanesulfonate; gold(I) chloride in 1,2-dichloro-ethane T=50°C; 3.5 h;
参考文献
Harrison, Tyler J.; Kozak, Jennifer A.; Corbella-Pane, Montserrat; Dake, Gregory R.
Journal of Organic Chemistry, 2006 , vol. 71, # 12 p. 4525 - 4529
19823-75-7
+
100-46-9
苄胺
→
反应条件
93026-61-0
反应条件
in toluene 2 h; Heating;
参考文献
Arcadi, Antonio; Rossi, Elisabetta
Tetrahedron, 1998 , vol. 54, # 50 p. 15253 - 15272
53626-84-9
+
100-46-9
苄胺
→
反应条件
93026-61-0
反应条件
ammonium acetate; potassium phosphate; copper(l) iodide; glycine-N',N'-dimethylamide hydrochloride in acetonitrile 20 h; Heating;
参考文献
Pan, Yuanjia; Lu, Hongjian; Fang, Yewen; Fang, Xinqiang; Chen, Liqun; Qian, Junlu; Wang, Junhua; Li, Chaozhong
Synthesis, 2007 , # 8 p. 1242 - 1246
17392-07-3
+
100-46-9
苄胺
→
反应条件
93026-61-0
反应条件
ammonium acetate; potassium phosphate; copper(l) iodide; glycine-N',N'-dimethylamide hydrochloride in toluene Heating;
参考文献
Pan, Yuanjia; Lu, Hongjian; Fang, Yewen; Fang, Xinqiang; Chen, Liqun; Qian, Junlu; Wang, Junhua; Li, Chaozhong
Synthesis, 2007 , # 8 p. 1242 - 1246
108-94-1
环己酮
→
反应条件
93026-61-0
反应条件
1.1: diisopropylamine; n-BuLi / tetrahydrofuran; hexane / 0.75 h 1.2: 83 percent / tetrahydrofuran; hexane / 3 h / 20 °C 2.1: 86 percent / triphenylphosphine / gold (I) chloride; silver (I) trifluoromathanesulfonate / 1,2-dichloro-ethane / 3.5 h / 50 °C View Scheme
参考文献
Harrison, Tyler J.; Kozak, Jennifer A.; Corbella-Pane, Montserrat; Dake, Gregory R.
Journal of Organic Chemistry, 2006 , vol. 71, # 12 p. 4525 - 4529
86953-53-9
→
反应条件
93026-61-0
反应条件
ammonium acetate; potassium phosphate; copper(l) iodide; glycine-N',N'-dimethylamide hydrochloride in acetonitrile Heating;
参考文献
Pan, Yuanjia; Lu, Hongjian; Fang, Yewen; Fang, Xinqiang; Chen, Liqun; Qian, Junlu; Wang, Junhua; Li, Chaozhong
Synthesis, 2007 , # 8 p. 1242 - 1246
53626-84-9
→
反应条件
93026-61-0
反应条件
1: TsOH / benzene 2: K3PO4; ammonium acetate / CuI; N,N-dimethylglycine hydrochloride / acetonitrile / Heating View Scheme
参考文献
Pan, Yuanjia; Lu, Hongjian; Fang, Yewen; Fang, Xinqiang; Chen, Liqun; Qian, Junlu; Wang, Junhua; Li, Chaozhong
Synthesis, 2007 , # 8 p. 1242 - 1246
100-46-9
苄胺
→
反应条件
93026-61-0
反应条件
1: TsOH / benzene 2: K3PO4; ammonium acetate / CuI; N,N-dimethylglycine hydrochloride / acetonitrile / Heating View Scheme
参考文献
Pan, Yuanjia; Lu, Hongjian; Fang, Yewen; Fang, Xinqiang; Chen, Liqun; Qian, Junlu; Wang, Junhua; Li, Chaozhong
Synthesis, 2007 , # 8 p. 1242 - 1246
1125-99-1
1-吡咯烷-1-环己烯
+
100-46-9
苄胺
+
513-31-5
2,3-二溴-1-丙烯
→
反应条件
93026-61-0
反应条件
1: 1-cyclohex-1-enylpyrrolidine; 1,2-dibromo-2-propene in 1,4-dioxane Heating; 2: benzylamine in toluene Heating;
参考文献
Tanyeli, Cihangir; Akhmedov, Idris M.; Yazicioglu, Emre Y.
Tetrahedron Letters, 2004 , vol. 45, # 52 p. 9627 - 9629
4471-09-4
→
反应条件
93026-61-0
反应条件
2: acetonitrile / 15 h / Heating View Scheme
参考文献
Ahlbrecht, Hubertus; Daacke, Axel von
Synthesis, 1984 , # 7 p. 610 - 614
