反应条件
in 1-Propyl acetate byproducts: CO2, Hg; to a boiling mixt. of acylate and solvent a soln. of peroxide was added, mixt. was heated and stirred (17 h); solvent was removed, residue was dissolved in EtOH, aq. KCl was added and mixt. was heated, alcohol was removed, chlorides were sepd., ppt. waswashed with hot acetic acid, residue was recrystd. from acetone, chromd;
参考文献
Ol'dekop, Yu. A.; Maier, N. A.; Erdman, A. A.; But'ko, Yu. D.
Journal of Organometallic Chemistry, 1980 , vol. 201, p. 39 - 46
