1,2,4,5-四氯苯合成路线 (共 206 条)
反应条件
beim Erhitzen auf Siedetemperatur;
参考文献
Journal of the Chemical Society, , p. 372
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 127, p. 1026
参考文献
Journal of the Chemical Society, , vol. 121, p. 1019
参考文献
Annales de Chimie (Cachan, France), , vol. <4> 15, p. 257
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, , p. 347
反应条件
aluminium trichloride T=160°C; 0.75 h;
参考文献
Ballester, Manuel; Riera, Juan; Castaner, Juan; Rovira, Concepcion; Armet, Olag
Synthesis, 1986 , # 1 p. 64 - 66
反应条件
aluminium trichloride Friedel-Crafts reaction;
参考文献
Mesa, Juan Antonio; Velazquez-Palenzuela, Amado; Brillas, Enric; Torres, Josep Lluis; Julia, Luis
Tetrahedron, 2011 , vol. 67, # 17 p. 3119 - 3123
反应条件
tetrabutylammomium bromide in N,N-dimethyl-formamide T=-5 - 0°C; Dehalogenation; Carboxylation; Electrochemical reaction; Further byproducts given;
参考文献
Golinske, Dirk; Voss, Juergen; Adiwidjaja, Gunadi
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 6 p. 862 - 880
反应条件
PdCl(C3H5)(1,4-bis(diphenylphosphino)butane); potassium acetate in N,N-dimethyl acetamide T=150°C; 20 h; Inert atmosphereSchlenk technique; regioselective reaction;
参考文献
Zhao, Liqin; Yan, Tao; Bruneau, Christian; Doucet, Henri
Catalysis Science and Technology, 2014 , vol. 4, # 2 p. 352 - 360
反应条件
1: bromobenzene With n-butyllithium in tetrahydrofuran; hexane 0.333333 h; cooling; 2: With zinc(II) chloride in tetrahydrofuran; hexane T=20°C; 0.333333 h; 3: 1,2,4,5-TeCB With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane Negishi coupling; 24 h; Heating;
参考文献
Russian Chemical Bulletin, , vol. 54, # 4 p. 970 - 974
反应条件
tetrabutylammomium bromide in N,N-dimethyl-formamide T=-5 - 0°C; Dehalogenation; Carboxylation; Electrochemical reaction; Further byproducts given;
参考文献
Golinske, Dirk; Voss, Juergen; Adiwidjaja, Gunadi
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 6 p. 862 - 880