1,3-二氯-2-丙醇合成路线 (共 217 条)
反应条件
hydrogenchloride T=93 - 120°C; P=5414.51 - 6965.99 Torr; 1.5 h; Product distribution / selectivity;
参考文献
WO2006/20234 A1, ;
Page/Page column 29-30 ;
反应条件
hydrogenchloride in water T=90°C; P=1794.37 - 5931.67 Torr; 2 h; Product distribution / selectivity;
参考文献
WO2006/20234 A1, ;
Page/Page column 38 ;
反应条件
hydrogenchloride; acetic acid T=105°C; P=975.098 Torr; 5.5 h; Product distribution / selectivity;
参考文献
WO2009/104961 A2, ;
Page/Page column 13-14 ;
反应条件
1: T=50 - 120°C; 2: With hydrogenchloride T=60°C;
参考文献
WO2011/93695 A1, ;
Page/Page column title page; 4 ;
反应条件
hydrogenchloride T=90 - 123°C; P=5414.51 - 5724.8 Torr; 1.5 - 2 h; Product distribution / selectivity;
参考文献
WO2006/20234 A1, ;
Page/Page column 35-37 ;
反应条件
sodium tetrahydroborate in methanol; dichloromethane 1 h; Ambient temperature;
参考文献
O'Hagan; White; Jones
Journal of Labelled Compounds and Radiopharmaceuticals, 1994 , vol. 34, # 9 p. 871 - 880
反应条件
hydrogenchloride in diethyl ether T=20°C; 1 h;
参考文献
Synlett, , # 6 p. 849 - 851
反应条件
hydrogenchloride; tert-butyl methyl ether; dimeric chiral (salen)Co complex linked with Al in diethyl ether T=0 - 5°C; 2 h; Product distribution; Further Variations:Catalysts;
参考文献
Thakur, Santosh Singh; Li, Wenji; Kim, Seong-Jin; Kim, Geon-Joong
Tetrahedron Letters, 2005 , vol. 46, # 13 p. 2263 - 2266
反应条件
hydrogenchloride T=110°C; P=2828.7 - 4690.48 Torr; 3 h; Product distribution / selectivity;
参考文献
WO2006/20234 A1, ;
Page/Page column 29-30 ;
反应条件
MgBr2(Et2O) in diethyl ether 9 h;
参考文献
Synthesis, , # 8 p. 647 - 649