potassium hydroxide; oxygen; PEG-400 in toluene T=25°C; 1 h; ultrasonic radiation; other catalysts, base; also for o-nitrotoluene, o-ethylnitrobenzene and p-ethylnitrobenzene; Product distribution;
参考文献
Neumann, Ronny; Sasson, Yoel
Journal of the Chemical Society, Chemical Communications, 1985 , # 9 p. 616 - 617
1.1: bromine; iron / chloroform / 48 h / 40 °C / Reflux 2.1: SnCl2·2H2O / ethanol; tetrahydrofuran / 3 h / 20 °C 2.2: 1.5 h 3.1: hydrogenchloride / water / 0.33 h 3.2: 2 h / 0 - 5 °C 3.3: 0 - 20 °C 4.1: tert.-butyl lithium / pentane; tetrahydrofuran / 2 h / -80 - -76 °C 4.2: -80 °C 4.3: pH 1 View Scheme
