in further solvent(s) byproducts: SO2, Cl2, HCl; refluxing PCl5 and (NH4)2SO4 in 1,1,2,2-tetrachloroethane for 12 h; cooling, washing with CCl4 or petroleum ether, elem. anal.;
参考文献
Helioui, Moncef; Chakra, Taher Abou; Jaeger, Roger de; Heubel, Joseph
Revue de Chimie Minerale, 1983 , vol. 20, p. 45 - 53
ethanol in 1,4-dioxane byproducts: Cl2(O)PN(C2H5)P(O)Cl2, POCl2(OC2H5), (C2H5O)Cl2PNP(O)Cl2; addn. of EtOH in dioxane to suspn. of (Cl3PNPCl3)PCl6 in dioxane (molar ratio 2:1) at ambient temp. during 1 h; not isolated; (31)P-NMR spectroscopic monitoring;
参考文献
Phosphorus, Sulfur, and Silicon and the Related Elements, , vol. 63, p. 19 - 32
