in tetrahydrofuran (N2); B complex added to a soln. of Rh complex and (C2H5)3N, shaken, heated at 50°C for 20 h; not isolated, detected by NMR;
参考文献
Mock, Michael T.; Potter, Robert G.; Camaioni, Donald M.; Li, Jun; Dougherty, William G.; Kassel, W. Scott; Twamley, Brendan; DuBois, Daniel L.
Journal of the American Chemical Society, 2009 , vol. 131, # 40 p. 14454 - 14465
in tetrahydrofuran under N2 or Ar, ice-acetone bath, -78°C, dropwise addn. of BF3*(C2H5)2O, stirred for 12 h, 25°C; filtered under N2, solvent removed in vac., distillation;
参考文献
Eisch, John J.; Shafii, Babak; Odom, Jerome D.; Rheingold, Arnold L.
Journal of the American Chemical Society, 1990 , vol. 112, # 5 p. 1847 - 1853
in diethyl ether addn. of MesMgBr in Et2O over a period of 1.5 h to BF3 in Et2O, refluxed for 3 h; removal of solvent in vac., sublimation (100°C, 1E-1 Torr);
参考文献
Chisholm, Malcolm H.; Folting, Kirsten; Haubrich, Scott T.; Martin, James D.
Inorganica Chimica Acta, 1993 , vol. 213, p. 17 - 24
