in water; diethylene glycol byproducts: NaBr, H2; NaBH4 in diglyme heated to 105°C, n-amyl bromide added to stirred suspn. over 5 h, suspn. allowed to cool, filtered, solids washed with Et2O, combined solns. evapd. residue dissolved in water and Me4NCl added; ppt. filtered and recrystd. from acetone/water;
参考文献
Dunks, Gary B.; Barker, Kathryn; Hedaya, Eddie; Hefner, Catherine; Palmer-Ordonez, Kathy; Remec, Peter
Inorganic Chemistry, 1981 , vol. 20, p. 1692 - 1697
aluminum tri-bromide in dichloromethane T=20°C; 0.25 h;
参考文献
Bolestova, G. I.; Parnes, Z. N.; Latypova, F. M.; Kursanov, D. N.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 7 p. 1203 - 1208
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 7 p. 1357 - 1363
