反应条件
1: 1.) tri-phenyl phosphine, 2.) aq. K2CO3 / 1.) MeCN, reflux, 5 h, 2.) MeCN, reflux, 6 h 2: aq. HCl / 4 h / Ambient temperature 3: H2 / 10percent Pd/C / ethyl acetate / 6 h / Ambient temperature 4: lithium aluminum hydride / tetrahydrofuran / 4 h / Ambient temperature 5: 90 percent / triethyl orthoformate, benzoic acid 6: pyridine / 15 h / -5 °C 7: NaI, Zn / various solvent(s) / 2 h / Heating View Scheme
参考文献
Bhushan, Kumar Hari; Rastogi, Archana; Subramanin, G.B.V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 10 p. 966 - 970
