反应条件
in ethylene glycol dimethyl ether byproducts: CO; N2-atmosphere; addn. of LiC5Me5 to mixt. of P-ligands (stirring), FeCl2 addn., stirring at room temp. for 16 h, solvent removal (vac.), chromy. (SiO2, hexane), dissoln. in CH2Cl2, addn. of Ni(CO)4 at 0°C, stirring at room temp. for 4 h; removal of volatiles (vac.), extn. into hexane, chromy. ((SiO2, hexane),recrystn. (hexane); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 512, # 1-2 p. 141 - 148
