2,5-二甲基-3-己炔-2,5-二醇合成路线 （共 93 条）
反应条件
sodium acetate; copper dichloride; palladium dichloride T=16°C; 4 h; influence of reaction conditions on yield; other reagents; in the absence of palladium; Product distribution;
参考文献
Trofimov; Mal'kina; Gritsa; Skvortsov; Stankevich; Sokolyanskaya
Russian Journal of General Chemistry, 1996 , vol. 66, # 1 p. 102 - 106
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 61, p. 1697
Chem. Zentralbl., , vol. 101, # I p. 3170
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 80
Chem.Abstr., , p. 7413
参考文献
Zhurnal Obshchei Khimii, , vol. 11, p. 939,945
Chem.Abstr., , p. 355
参考文献
Justus Liebigs Annalen der Chemie, , vol. 442, p. 80
Chemische Berichte, , vol. 55, p. 2909
参考文献
Zhurnal Obshchei Khimii, , vol. 11, p. 939,945
Chem.Abstr., , p. 355
反应条件
bis-triphenylphosphine-palladium(II) chloride in benzene T=90 - 100°C; 25 h; further catalysts, reagent concentrations, reaction time; Product distribution;
参考文献
Kiji, Jitsou; Konishi, Hisatoshi; Okano, Tamon; Kometani, Shinji; Iwasa, Akio
Chemistry Letters, 1987 , p. 313 - 314
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 1.) 0 deg C, 30 min, 2.) reflux, 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Huang, Jiling; Goedken, V.; Walborsky, H. M.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4128 - 4131
反应条件
palladium on activated charcoal Hydrogenation;
参考文献
Tedeschi,R.J.
Journal of Organic Chemistry, 1962 , vol. 27, p. 2398 - 2402
反应条件
bei der katalytischen Hydrierung entstehen je nach den Bedingungen verschiedene Produkte.Hydrogenation;
参考文献
Dupont
Annales de Chimie (Cachan, France), 1913 , vol. <8> 30, p. 539,583
Full Text Show Details
Salkind
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1913 , vol. 45, p. 1883
Chem. Zentralbl., 1914 , vol. 85, # I p. 1813
