反应条件
AlCl3; Al; HCl in 2-methyl cyclohexane (N2); addn. of methylcyclohexane to a mixt. of ligand, ferrocene, AlCl3,Al, heating to 40°C, addn. of TiCl4, heating to 100°C, st irring for 1 h, addn. to aq. HCl, heating to 50°C, cooling, addn.of aq. KPF6, stirring for 30 min; filtration, evapn., dissolving in acetone, drying (MgSO4), filtration, addn. of Et2O;
参考文献
Kuendig, E. Peter; Jeger, Patrick; Bernardinelli, Gerald
Inorganica Chimica Acta, 2004 , vol. 357, # 6 p. 1909 - 1919
