1: n-butyl-triphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane
T=-15°C;
2: 4-fluoro-N-methoxy-N-methyl-benzamide in tetrahydrofuran; hexane
T=-78 - 20°C; Wittig reaction;
3: With hydrogenchloride in tetrahydrofuran; diethyl ether; hexane
T=20°C;
参考文献
Murphy, John A.; Commeureuc, Aurelien G. J.; Snaddon, Thomas N.; McGuire, Thomas M.; Khan, Tanweer A.; Hisler, Kevin; Dewis, Mark L.; Carling, Robert
Organic Letters, 2005 , vol. 7, # 7 p. 1427 - 1429
water; potassium carbonate in benzene
T=70°C; 6 h; further basic reagents; effect of water addition; further solvents, temperatures; futrher aldehydes; Product distributionMechanism;
参考文献
Le Bigot, Yves; Delmas, Michel; Gaset, Antoine
Tetrahedron, 1988 , vol. 44, # 4 p. 1057 - 1072
