4-苯基-3-丁炔-2-酮合成路线 (共 131 条)
反应条件
1: diluted alcohol 2: 100 °C / im Rohr View Scheme
参考文献
v. Auwers; Stuhlmann
Chemische Berichte, 1926 , vol. 59, p. 1054
反应条件
1: ammonium hydroxide / ethanol / 7 h / Heating 2: 81 percent View Scheme
参考文献
Liso, Gaetano; Trapani, Giuseppe; Reho, Antonia; Latrofa, Andrea; Loiodice, Fulvio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 567 - 572
反应条件
sodium hydride in 1,4-dioxane; N,N-dimethyl-formamide 1.) r.t., 0.5 h, 2.) 0.5 h;
参考文献
Gomez, Virginia; Perez-Medrano, Arturo; Muchowski, Joseph M.
Journal of Organic Chemistry, 1994 , vol. 59, # 5 p. 1219 - 1221
参考文献
Andre
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1911 , vol. 152, p. 1489
Annales de Chimie (Cachan, France), 1913 , vol. <8> 29, p. 581
反应条件
sodium hydroxide; ethylenediaminetetraacetic acid; dihydrogen peroxide in water T=25°C; 10 h; mechanism; energy data: ΔH(excit.), ΔS(excit.); other electron deficient acetylenes and related compounds, other alcohol, var. temp. and reagent ratio; KineticsRate constantProduct distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 56, # 4 p. 1133 - 1138
反应条件
Behandlung des Reaktionsproduktes mit krystallwasserhaltiger Oxalsaeure in Aether;
参考文献
Andre
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1911 , vol. 152, p. 1489
Annales de Chimie (Cachan, France), 1913 , vol. <8> 29, p. 581
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 325
反应条件
NB-Enantride in tetrahydrofuran; diethyl ether; pentane T=-100°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 47, # 12 p. 2495 - 2496
反应条件
titanium(IV) isopropylate; 2,2'-azo-bisisobutyronitrile; tetranaphthyl-TADDOL; Ph2SbH in hexane 16 h; Heating;
参考文献
Journal of Organometallic Chemistry, , vol. 571, # 2 p. 297 - 303
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); gold(I) chloride in acetonitrile T=85°C;
参考文献
Schuler, Marie; Silva, Franck; Bobbio, Carla; Tessier, Arnaud; Gouverneur, Veronique
Angewandte Chemie - International Edition, 2008 , vol. 47, # 41 p. 7927 - 7930