9-硼二环[3.3.1]壬烷 二聚物合成路线 （共 39 条）
反应条件
(Z,Z)-1,5-cyclooctadiene COD and THF*BH3, mole ratio 1:1, at 65°C;;
参考文献
Gmelin Handbook: B: B-Verb.14, 5.6, page 212 - 224
反应条件
in ethylene glycol dimethyl ether T=20°C; Inert atmosphere;
参考文献
Soderquist, John A.; Kock, Iveliz; Estrella, Maria E.
Organic Process Research and Development, 2006 , vol. 10, # 5 p. 1076 - 1079
反应条件
(Z,Z)-1,5-cyclooctadiene COD and ((C2H5)2BH)2, mole ratio 2:3;;
参考文献
Gmelin Handbook: B: B-Verb.14, 5.6, page 212 - 224
反应条件
lithium aluminium tetrahydride isolation by trapping with 1-octene;;
参考文献
Journal of the American Chemical Society, , vol. 92, p. 6648 - 6649
反应条件
in diethyl ether byproducts: H2, KCl; under inert atm. soln. K(H2BC8H14) in Et2O was added dropwise to soln. TiCl4 in Et2O (5:1) and stirred at room temp. for 12 h; soln. was filtered and evapd. in vacuo, residue was dissolved in ether and kept at -30°C; elem. anal.;
参考文献
Ding, Errun; Du, Bin; Liu, Fu-Chen; Liu, Shengming; Meyers, Edward A.; Shore, Sheldon G.
Inorganic Chemistry, 2005 , vol. 44, # 13 p. 4871 - 4878
反应条件
in diethyl ether (N2); drybox; mixt. of Zr complex and B(C6F5)3 in ether was stirred for 1 h; NMR monitoring; filtered;
参考文献
Organometallics, , vol. 23, # 9 p. 2100 - 2106
反应条件
in hexane N2, a soln. of Ti comp. added to a suspn. of B compd., stirred for 2 d; filtered, concd., stored at -30°C for several d; elem. anal.;
参考文献
European Journal of Inorganic Chemistry, , # 12 p. 1888 - 1900
参考文献
Angewandte Chemie, , vol. 72, p. 626 - 627
Journal of the American Chemical Society, , vol. 90, p. 5280 - 5281
Inorganic Syntheses, , vol. 15, p. 141 - 149
B: B-Verb.14, 4.3.3.3, page 182 - 183
反应条件
(Z,Z)-1,5-cyclooctadiene in neat (no solvent) heating mixt. at 65°C; distn. of B(C2H5)3; recrystn. from heptane;;
参考文献
Inorganic Syntheses, , vol. 15, p. 141 - 149
Organic Syntheses via Boranes, John Wiley and Sons, New York - London - Sydney - Toronto 1975
参考文献
Journal of the American Chemical Society, , vol. 96, p. 7765 - 7770
Journal of the American Chemical Society, , vol. 90, p. 5280 - 5281
B: B-Verb.14, 4.3.3.3, page 182 - 183
