2-壬烯 (顺反异构体混合物)合成路线 （共 10 条）
反应条件
Pd[P(t-Bu)3]2 in toluene T=20°C; Schlenk techniqueInert atmosphere;
参考文献
Giannerini, Massimo; Fananas-Mastral, Martin; Feringa, Ben L.
Nature Chemistry, 2013 , vol. 5, # 8 p. 667 - 672
反应条件
tri-isobutyl aluminium; bis(cyclopentadienyl)titanium dichloride T=90°C; Inert atmosphereSealed vial;
参考文献
DOW GLOBAL TECHNOLOGIES LLC; CLARK, Thomas, P.; FRAZIER, Kevin, A.; TIMMERS, Francis, J.; KOLTHAMMER, Brian, W.
Patent: WO2011/81650 A1, 2011 ;
Location in patent: Page/Page column 5-6 ;
反应条件
hydrogen; H-ZSM-5 T=189.84°C; P=26252.6 Torr; Product distribution / selectivity;
参考文献
Dumesic, James A.; Ruiz, Juan Carlos Serrano; West, Ryan M.
Patent: US2010/324310 A1, 2010 ;
Location in patent: Page/Page column 14 ;
反应条件
rhenium(VII) oxide on aluminum oxide in supercritical CO2 T=35°C; Self-metathesis; P=67506.8 Torr; 2 h; Inert atmosphereAutoclave; chemoselective reaction;
参考文献
Selva, Maurizio; Perosa, Alvise; Fabris, Massimo; Canton, Patrizia
Green Chemistry, 2009 , vol. 11, # 2 p. 229 - 238
反应条件
1: With bis(cyclopentadienyl)titanium dichloride; ethylaluminum dichloride; magnesium in tetrahydrofuran T=0 - 20°C; 2: With hydrogenchloride in tetrahydrofuran
参考文献
Ibragimov; Khafizova; Gil'fanova; Dzhemilev
Russian Chemical Bulletin, 2002 , vol. 51, # 12 p. 2255 - 2260
反应条件
tri-ruthenium(0)dodecacarbonyl; water; triphenylphosphine in N,N-dimethyl-formamide T=130°C; 12 h; AutoclaveGreen chemistry; Temperature;
参考文献
Karakhanov, Eduard; Maksimov, Anton; Kardasheva, Yulia; Runova, Elena; Zakharov, Roman; Terenina, Maria; Kenneally, Corey; Arredondo, Victor
Catalysis Science and Technology, 2014 , vol. 4, # 2 p. 540 - 547
反应条件
tri-ruthenium(0)dodecacarbonyl; water; triphenylphosphine in N,N-dimethyl-formamide T=130°C; 12 h; AutoclaveGreen chemistry; Temperature;
参考文献
Karakhanov, Eduard; Maksimov, Anton; Kardasheva, Yulia; Runova, Elena; Zakharov, Roman; Terenina, Maria; Kenneally, Corey; Arredondo, Victor
Catalysis Science and Technology, 2014 , vol. 4, # 2 p. 540 - 547
反应条件
P(O-4-C6H4C6F13)3; hydrogen; [rhodium(I)(carbonyl)2(acetylacetonate)] in various solvent(s) T=70°C; P=15001.2 Torr; 1 h; Product distributionKinetics;
参考文献
Foster, Douglas F; Gudmunsen, David; Adams, Dave J; Stuart, Alison M; Hope, Eric G; Cole-Hamilton, David J; Schwarz, Gary P; Pogorzelec, Peter
Tetrahedron, 2002 , vol. 58, # 20 p. 3901 - 3910
反应条件
oxygen; palladium diacetate; toluene-4-sulfonic acid in water T=100°C; P=6080.41 Torr; 24 h; Autoclave;
参考文献
Journal of Organic Chemistry, , vol. 75, # 7 p. 2321 - 2326
反应条件
P(O-4-C6H4C6F13)3; hydrogen; [rhodium(I)(carbonyl)2(acetylacetonate)] in various solvent(s)
T=70°C; P=15001.2 Torr; 1 h; Product distributionKinetics;
参考文献
Foster, Douglas F; Gudmunsen, David; Adams, Dave J; Stuart, Alison M; Hope, Eric G; Cole-Hamilton, David J; Schwarz, Gary P; Pogorzelec, Peter
Tetrahedron, 2002 , vol. 58, # 20 p. 3901 - 3910
