1: 1,3-Dithiane With n-butyllithium; diisopropylamine in tetrahydrofuran
T=-78°C; 0.5 h;
2: diethyl chlorophosphate in tetrahydrofuran
T=-78°C; 1 h; Further stages.;
参考文献
Liu, Bin; Duan, Shengquan; Sutterer, Angela C.; Moeller, Kevin D.
Journal of the American Chemical Society, 2002 , vol. 124, # 34 p. 10101 - 10111
Hwu, Jih Ru; Lee, Taekyo; Gilbert, Bryant A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 23 p. 3219 - 3224