1-苯基戊烷-1,3-二酮合成路线 （共 36 条）
反应条件
sodium ethanolate
Heating;
参考文献
Jezierska, Aneta; Jerzykiewicz, Lucjan B.; Kolodziejczak, Jerzy; Sobczak, Jaroslaw M.
Journal of Molecular Structure, 2007 , vol. 839, # 1-3 p. 33 - 40
反应条件
(i) TsOH, (ii) NaNH2; Multistep reaction;
参考文献
Muir,W.M. et al.
Journal of Organic Chemistry, 1966 , vol. 31, p. 3790 - 3793
反应条件
(i) LDA, Et2O, THF, (ii) /BRN= 1761272/; Multistep reaction;
参考文献
Couffignal,R.; Moreau,J.-L.
Journal of Organometallic Chemistry, 1977 , vol. 127, p. C65 - C68
反应条件
T=0°C; anschliessendes Erwaermen des Reaktionsgemisches;
参考文献
Morgan; Drew; Porter
Chemische Berichte, 1925 , vol. 58, p. 333,336
反应条件
Behandlung des Reaktionsproduktes mit krystallwasserhaltiger Oxalsaeure in Aether;
参考文献
Andre
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1911 , vol. 152, p. 1489
Annales de Chimie (Cachan, France), 1913 , vol. <8> 29, p. 581
参考文献
Moureu; Brachin
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1904 , vol. 139, p. 209
Bulletin de la Societe Chimique de France, 1905 , vol. <3> 33, p. 137,141
反应条件
Behandeln des Reaktionsgemisches mit wss. Salzsaeure;
参考文献
Mavrodin
Bulet. Soc. Chim. Romania, 1933 , vol. 15, p. 99,102
反应条件
iodine; oxygen; Ca(OH)2 in ethyl acetate
10 h; photoirradiation;
参考文献
Tada, Norihiro; Shomura, Motoki; Nakayama, Hiroki; Miura, Tsuyoshi; Itoh, Akichika
Synlett, 2010 , # 13 p. 1979 - 1983
反应条件
anhydrous iron chloride; tert.-butylnitrite
T=30°C; 12 h; Under airNeat (no solvent);
参考文献
Huang, Lehao; Cheng, Kai; Yao, Bangben; Xie, Yongju; Zhang, Yuhong
Journal of Organic Chemistry, 2011 , vol. 76, # 14 p. 5732 - 5737
反应条件
1: 70 percent / conc. HCl / ethanol / 48 h / Heating
2: 85 percent / phosphoryl chloride / 3 h / Heating
3: 96 percent / hydrogen/conc. ammonia / 5percent palladium charcoal / methanol
View Scheme
参考文献
Sakamoto, Takao; Sakasai, Takeji; Yoshizawa, Hiroshi; Tanji, Ken-Ichi; Nishimura, Sumiko; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4554 - 4560
