1,3-苯并二硫代吡咯四氟化硼盐合成路线 (共 20 条)
反应条件
triphenylmethane tetrafluoroborate in acetonitrile T=0 - 3°C; 0.5 h;
参考文献
Nakayama, Juzo; Fujiwara, Kazuo; Hoshino, Masamatsu
Journal of Organic Chemistry, 1980 , vol. 45, p. 2024 - 2025
反应条件
tetrafluoroboric acid in acetic anhydride
参考文献
Tetrahedron, , vol. 59, # 33 p. 6353 - 6362
反应条件
Ambient temperature;
参考文献
Nakayama, Juzo; Sugie, Yasuko; Hoshino, Masamatsu
Chemistry Letters, 1987 , p. 939 - 940
反应条件
chlorine in chloroform; water; tert-butyl alcohol T=0 - 5°C;
参考文献
Barbero, Margherita; Degani, Iacopo; Fochi, Rita; Regondi, Valeria
Gazzetta Chimica Italiana, 1986 , vol. 116, # 3 p. 165 - 166
反应条件
sodium iodide in acetonitrile Heating;
参考文献
Tetrahedron, , vol. 59, # 33 p. 6353 - 6362
反应条件
sodium tetrahydroborate in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Boyd, Derek R.; Sharma, Narain D.; Dorman, James H.; Dunlop, Robert; Malone, John F.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 9 p. 1105 - 1110
反应条件
1: acetonitrile / 16 h / 80 °C / |Inert atmosphere
2: sodium tetrahydroborate / tetrahydrofuran / 1 h / 0 °C / |Inert atmosphere
View Scheme
参考文献
Petruzziello, Diego; Gualandi, Andrea; Jaffar, Hamza; Lopez-Carrillo, Veronica; Cozzi, Pier Giorgio
European Journal of Organic Chemistry, 2013 , # 22 p. 4909 - 4917
反应条件
in acetonitrile
T=80°C; Inert atmosphere;
参考文献
Petruzziello, Diego; Gualandi, Andrea; Jaffar, Hamza; Lopez-Carrillo, Veronica; Cozzi, Pier Giorgio
European Journal of Organic Chemistry, 2013 , # 22 p. 4909 - 4917
反应条件
in dichloromethane
24 h; Ambient temperature;
参考文献
Nakayama, Juzo; Sugie, Yasuko; Hoshino, Masamatsu
Chemistry Letters, 1987 , p. 939 - 940
反应条件
in dichloromethane
1.5 h; Ambient temperature;
参考文献
Nakayama, Juzo; Sugie, Yasuko; Hoshino, Masamatsu
Chemistry Letters, 1987 , p. 939 - 940