1H-imidazole; iodine; triphenylphosphine in dichloromethane T=20°C; Inert atmosphereCooling with ice;
参考文献
Ren, Peng; Vechorkin, Oleg; Von Allmen, Kim; Scopelliti, Rosario; Hu, Xile
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 7084 - 7095
1: cis-3-hexanol With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene in dichloromethane 16 h; 2: benzylamine With sodium tris(acetoxy)borohydride in dichloromethane chemoselective reaction;